1-Bromohexane
-
- Category :
Intermediates/Pharmaceutical intermediates
- CAS NO : 111-25-1
- EC NO : 203-850-2
- Molecular Formula : C6H13Br
- Main Specifications : 99% min
- Synonyms : n-Hexyl bromide;Bromohexane;HEXYL BROMIDE;Bromohexane;N-BROMOHEXANE;1-bromo-hexan;1-Hexyl bromide;1-hexylbromide;1-bromo hexane;n-Hexylbromide;
Package: 25kg，50kg 200kg
Uses : As an intermediate in organic synthesis
Molecular Structure:
Product description:
What is the chemical of 1-Bromohexane ?
Appearance: Colorless to pale yellow transparent oily liquid ;
Assay：99%min by GC ;
IR Identity: conform to standard ;
HNMR： conform to standard ;
carbon spectrum: conform to standard ;
Water by K. F.:0.5% max or as per the customer’s request ;
Loss on drying:0.5% max. or as per the customer’s request ;
boiling point: 154–158 °C;
===========================================================================
Main purpose:
Used as an organic solvent;
As an intermediate in organic synthesis, it is used to prepare other organic compounds;
It is the raw material for preparing polyketide ionic liquids
============================================================================
Synthesis route (preparation method)
According to publicly available information, a common laboratory synthesis method is as follows
Dissolve 16 g (0.1 mol bromine) in 50 mL of carbon tetrachloride;
Slowly add dropwise with stirring to a mixture consisting of 13 g (0.1 mol heptanoic acid) and 22 g (0.0945 mol mercuric oxide) dissolved in 150 mL of dry carbon tetrachloride;
After reflux reaction, the filtrate was washed successively with 5% NaOH solution and water;
Dry with anhydrous sodium sulfate;
Fractionate the collected product to obtain approximately 6 g (36% yield) of 1-bromohexane.
Search Product